SpraySyn Database

Nanoparticle Synthesis in Spray Flames

166

Authors Name:

Munko Gonchikzhapov

Affliations:

University of Duisburg-Essen, Institute for Combustion and Gas Dynamics - Mass spectrometry in reacting flows, Germany

Date of Dataset Creation:

Feb. 10, 2020

Publication Reference:

M. Gonchikzhapov and T. Kasper, Decomposition Reactions of Fe(CO)5 and TTIP as Precursors for the Spray Flame Synthesis of Nanoparticles in Partial Spray Evaporation at Low Temperatures, Industrial and Engineering Chemistry Research, under revision

Embargo Time:

June 1, 2020

DataGeneration Type:

Experiment

Methods:

microprobe sampling, TOF-MS, micro thermocouple

Instruments:

Orthogonal Extraction Reflection Time-of-Flight mass-spectrometer

Software:

Excel, Origin

Models:

N/A

Device:

SpraySyn burner, tubular reactor

Configuration:

Spray decomposition: 0.8 mol/L precursor (IPC,TTIP, ferrocene), solvents: ethanol, o-xylene. Flame measurements: pilot premixed and burned 16 slm O2 + 2 slm CH4, dispersion flow - 10 slm.

Precursor:

titanium tetraisopropoxide (TTIP), Iron pentacarboy; (IPC), Ferrocene

Data Type:

Result Data

Variables:

main flame species, flame temperature

Error_Estimation:

20%